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五氟溴苯合成工艺研究
Study on the Sythesis Technics of Bromopentafluorobenzene
【摘要】 五氟溴苯是一种非常重要的化工中间体,五氟苯甲酸通过脱羧、溴化两步反应最终可得到五氟溴苯,分别研究了脱羧和溴化反应中各反应条件对目的产物收率的影响。
【Abstract】 Bromopentafluorobenzene is a very important fine chemical intermediate.In this paper bromopentafluorobenzene is synthetized from pentafluorobenzoic acid via decarboxylation and bromination in correct order,then the effects of reaction conditions,such as concentration and quantity of sulfuric acid,reaction temperature and time have been investigated separately.
【关键词】 五氟溴苯;
五氟苯甲酸;
脱羧反应;
溴化反应;
【Key words】 Bromopentafluorobenzene; Pentafluorobenzoic acid; Decarboxylation; Bromination;
【Key words】 Bromopentafluorobenzene; Pentafluorobenzoic acid; Decarboxylation; Bromination;
- 【文献出处】 上海化工 ,Shanghai Chemical Industry , 编辑部邮箱 ,2010年10期
- 【分类号】TQ242.1
- 【被引频次】1
- 【下载频次】240