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40%异稻·稻瘟灵乳油的气相色谱分析

Determination of Iprobenfos·Isoprothiolane 40% EC by GC

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【作者】 程运斌刘育清

【Author】 CHENG Yun-bin1,LIU Yu-qing2(1.Agricultural Testing & Information Center,Hubei Academy of Agricultural Sciences,Wuhan 430064,China;2.Institute for the Control of Agrochemicals of Hubei Province,Wuhan 430070,China)

【机构】 湖北省农科院农业测试与科技信息中心湖北省农药检定管理所

【摘要】 介绍了以5%OV-101色谱柱固定相、邻苯二甲酸二丁酯为内标物,用FID检测器对40%异稻?稻瘟灵乳油2种组分的气相色谱分离测定方法。结果表明:异稻瘟净和稻瘟灵的标准偏差分别为0.096、0.129,变异系数分别为0.32%、1.24%,异稻瘟净的回收率为98.94%~101.17%,稻瘟灵的回收率为98.97%~100.45%。

【Abstract】 A specific quantitative analysis method for iprobenfos.isoprothiolane 40% EC by GC was reported.The sample was separated in a column packed with 5% OV-101 using dibutyl phthalate as internal standard and detected by flame ionization detector.The results showed that the standard deviation for iprobenfos and isoprothiolane were 0.096 and 0.129,the coefficient of variation were 0.32 and 1.24%,the recoveries were between 98.94-101.17% and 98.97-100.45%.

【关键词】 异稻瘟净稻瘟灵气相色谱分析
【Key words】 iprobenfosisoprothiolanegas chromatographanalysis
  • 【分类号】TQ450.7
  • 【被引频次】1
  • 【下载频次】75
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