【摘要】 考察了催化剂及其加入量、溶剂及其加入量、反应温度、反应压力对邻硝基对叔丁基苯酚加氢反应的影响。适宜的条件为:催化剂:采用浸渍法制备的自制样,加入量0.10～0.15 g,溶剂:乙醇和正丁醇,优选正丁醇,加入量50 mL,反应温度90℃,反应压力0.10 MPa。更多还原

【Abstract】 Influences the kinds of catalyst and its addition amount,the kinds of solvent and its addition amount,the reaction temperature,and the reaction pressure on reaction of 2-nitro-4-tert-butyl-phenol catalytic hydrogenation were investigated.The suitable conditions were catalyst: the homemade catalyst by impregnation,its addition amount: 0.10～0.15 g;solvent: ethanol and n-butyl alcohol,optimization to n-butyl alcohol,its addition amount: 50 mL;the reaction temperature: 90 ℃;the reaction pressure: 0.10 MPa.更多还原