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正交试验法优选石墨炉测定大米中镉的实验条件

Application of Orthogonal Experimental Design in Optimization of Determination Conditions of Cadmium in Rice by GFAAS

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【作者】 张红艳王成秦国新肖英帕尔哈提田新玲

【Author】 ZHANG Hong-yan ,WANG Cheng ,QIN Guo-xin , XIAO Ying , PAER Ha-ti , TIAN Xin-ling(Test Centre , Xinjiang Academy of Agricultural Science, Urumqi 830000, China)

【机构】 新疆农科院测试中心

【摘要】 利用L16(45)正交试验设计,考察了石墨炉原子吸收法测定大米中镉的灰化温度、灰化时间、原子化温度、原子化时间.确定了最佳灰化温度为450℃、灰化时间为15s、原子化温度为1750℃、原子化时间为4s等仪器的最佳参数.

【Abstract】 Using the L16(45) orthogonal experimental design, factors including ashing temperature , ashing time ,atomization temperature, atomization time were studied in the determination of cadmium in rice by graphite furnace atomic absorption spectrometry. The instrument parameters were determined : the optimized ashing temperature, ashing time, atomization temperature, and atomization time were 450 ℃, 15 s, 1 750 ℃ and 4 s, respectively.

  • 【文献出处】 分析测试技术与仪器 ,Analysis and Testing Technology and Instruments , 编辑部邮箱 ,2010年04期
  • 【分类号】S511
  • 【下载频次】153
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