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二苄叉丙酮制备实验的改进
An improved experiment for preparation of bis-benzalacetone
【摘要】 该文对二苄叉丙酮的制备实验进行了改进。用分子筛固载氟化钾代替氢氧化钠作催化剂,研究了醛酮物质的量之比、催化剂用量和溶剂对产率的影响,确定了最佳合成条件。
【Abstract】 The experiment for preparation of bis-Benzalacetone has been improved by using KF supported on molecular sieve to substitute for NaCl as the catalyst.In order to determine the optimum synthesis condition,the paper studied the mol ratio of aldehyde and ketone and the affect of the amount of the catalyst and the solvent on productivity.
【关键词】 分子筛固载氟化钾;
Claisen-Schmidt缩合;
二苄叉丙酮;
α,α′-二取代苯叉丙酮;
【Key words】 KF supported on molecular sieve; Claisen-Schmidt condensation; bis-Benzalacetone; α,α′-dibenzylideneacetones;
【Key words】 KF supported on molecular sieve; Claisen-Schmidt condensation; bis-Benzalacetone; α,α′-dibenzylideneacetones;
【基金】 国家自然科学基金项目(项目编号:20772088);苏州大学高等教育教学改革(2007-16)
- 【文献出处】 实验室科学 ,Laboratory Science , 编辑部邮箱 ,2009年06期
- 【分类号】TQ244.2
- 【被引频次】2
- 【下载频次】1410