节点文献
热水解-离子选择电极法测定海相碳酸盐岩中的氟
Determination of Fluorine in Marine Carbonate Rocks by Pyrohydrolysis-Ion Selective Electrode Method
【摘要】 采用热水解法对样品进行预处理,离子选择电极法简易快速测定海相碳酸盐岩中氟元素的含量。方法检出限为25.1μg/g,精密度(RSD,n=11)为5.28%,回收率为96.5%~107.8%,结果令人满意。
【Abstract】 A method for the determination of fluorine in marine carbonate rocks by ion selective electrode with pyrohydrolysis sample pretreatment has been developed.The detection limit of the method is 25.1 μg/g for fluorine and the recovery is 83.80%~107.90% with precision of 5.28%RSD(n=11).The method has been applied to the determination of fluorine in marine carbonate rock samples with satisfactory results and provides the advantages of high efficiency and simple operation.
【关键词】 热水解;
离子选择电极法;
海相碳酸盐岩;
氟;
【Key words】 pyrohydrolysis; ion-selective electrode; marine carbonate rock; fluorine;
【Key words】 pyrohydrolysis; ion-selective electrode; marine carbonate rock; fluorine;
【基金】 中石化“海相优质烃源岩形成的地球生物学过程——烃源岩形成的生物地球化学记录及埋藏过程”项目资助(G0800-06-2S-319)
- 【文献出处】 岩矿测试 ,Rock and Mineral Analysis , 编辑部邮箱 ,2009年02期
- 【分类号】P575
- 【被引频次】14
- 【下载频次】132