【摘要】 通过微波辐射,以FeCl3为催化剂进行无溶剂条件下的呐醇重排反应,1min产率可达86%～96%.该方法具有操作简便、反应时间缩短、对环境友好等优点.更多还原

【Abstract】 The pinacol rearrangement catalysed by FeCl3 in the absence of solvent was carried out. The pinacolones were obtained in yields of 86%～96% for 1 min under microwave irradiation, which provided several advantages such as simple work-up procedure, shorter reaction time, and environmental friendliness.更多还原