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~1HNMR法定量测定亚氨基二苄的质量分数
Quantitative determination of iminodibenzyl by ~1HNMR
【摘要】 采用核磁共振(1HNMR)法测定了亚氨基二苄的质量分数,给出了最佳的实验条件和注意事项,线性实验测得线性回归系数为0.9998,精密度实验测得相对标准偏差为0.2105%~0.3262%.表明此方法作为一种化合物的定量测定具有简单易行、结果准确的优点,可作为某些难以获得对照品的化合物定量分析方法的补充.
【Abstract】 The quantitative determination of iminodibenzyl by 1HNMR has been developed in this paper.The optimum experimental conditions and some announcements have been described.As a method of medical quantitative determination,its efficacy has been proved through the experiments of precision and linearity.The coefficient of linear regression and RSD are 0.999 8 and 0.210 5%~0.326 2% respectively.This method is simple and accurate,and can be utilized as a supplement to the quantitative determination when without reference compounds.
【关键词】 1HNMR;
亚氨基二苄;
定量;
线性;
精密度;
【Key words】 1HNMR; iminodibenzyl; quantitative determination; linearity; precision;
【Key words】 1HNMR; iminodibenzyl; quantitative determination; linearity; precision;
【基金】 国家自然科学基金资助项目(20672090);徐州市科技局自然科学基金资助项目(XJ07066);江苏省大型科学仪器设备共享服务平台理事会资助项目;徐州师范大学自然科学基金资助项目(07XLB20)
- 【文献出处】 徐州师范大学学报(自然科学版) ,Journal of Xuzhou Normal University(Natural Science Edition) , 编辑部邮箱 ,2009年01期
- 【分类号】TQ207.4
- 【被引频次】1
- 【下载频次】76