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F掺杂SnO2纳米粉体的燃烧合成

Synthesis of Fluorine-Doped Tin Oxide Nanoparticles by Combustion Method

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【作者】 王海文徐秀娟李秀花张建荣高濂

【Author】 Wang Haiwen1 Xu Xiujuan1 Li Xiuhua1 Zhang Jianrong1,2 Gao Lian2(1Key Laboratory for Advanced Materials of Ministry of Education,East China University of Science and Technology,Shanghai 200237,2Shanghai Institute of Ceramics,Chinese Academy of Sciences,Shanghai 200050)

【机构】 华东理工大学先进材料教育部重点实验室中国科学院上海硅酸盐研究所

【摘要】 以金属锡和HF为原料采用燃烧合成法合成得到了F掺杂SnO2纳米颗粒。燃烧反应中甘氨酸为燃料,硝酸为氧化剂。采用XRD,BET,TEM和EDS等分析手段对合成得到的FTO进行了表征。结果显示,F的掺杂促进了SnO2基体晶粒的长大,所得到的粉体团聚较少,呈单分散状态。

【Abstract】 Nanocrystalline fluorine-doped tin oxide particles were synthesized by the combustion method from the starting material tin and fluorine acid.The fuel was glycine acid and the oxidant was HNO3.The nanoparticles were characterized by XRD,BET,TEM and EDS.The results revealed that the crystallite size of the FTO nanoparticles increased with the increase of fluorine doping level.The obtained nanoparticles were less agglomerated and monodispersed.

【关键词】 纳米粉体氧化锡掺杂
【Key words】 nanoparticletin oxidedoping
  • 【文献出处】 现代技术陶瓷 ,Advanced Ceramics , 编辑部邮箱 ,2009年04期
  • 【分类号】TB383.1
  • 【被引频次】2
  • 【下载频次】111
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