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木浆乙酰化工艺研究
Study on technology of acetylation of wood pulp
【摘要】 对木浆进行乙酰化,研究不同活化和酯化工艺对木浆乙酰化产物的影响,得出工艺条件为活化时间3 h、温度80℃、固液比1∶9;酯化时间2 h、温度50℃、催化剂用量2.50%以及反应摩尔比2.00的情况下,所得产物的不溶物含量较少,特性黏数较大,性能优良。
【Abstract】 The influence of activated and acetylaed technology on the production of acetylated wood pulp are investigated.The results show that under the conditions of activated time of 3 h,activated temperature of 80℃,amount of acid as 9 times to that of pulp,acetylated time of 2 h,acetylated temperature of 50℃,amount of sulfuric acid 2.50% and the molar rate of acetic anhydride as 2 times to that of the cellulose’s hydroxyl group,the product has good properties with less insoluble residues and fine intrinsic viscosity.
【关键词】 木浆;
乙酰化;
取代度;
不溶物;
特性黏数;
【Key words】 wood pulp; acetylation; degree of substitution; insoluble residue; intrinsic viscosity;
【Key words】 wood pulp; acetylation; degree of substitution; insoluble residue; intrinsic viscosity;
- 【文献出处】 现代化工 ,Modern Chemical Industry , 编辑部邮箱 ,2009年S2期
- 【分类号】TQ316.3
- 【被引频次】4
- 【下载频次】117