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静电自组装制备新型复合材料及其表征
Preparation of a Novel Composite Material Using the Electrostatic Self-assembly and Its Characterization
【摘要】 采用静电自组装及真空冷冻干燥技术,制备了聚乳酸(PDLLA)/硫酸软骨素(CS)/壳聚糖(CHS)新型复合材料。利用各种分析手段对材料进行了表征,包括用紫外可见光谱监测自组装过程;利用傅立叶变换红外光谱(FT-IR)和X-射线光电子能谱(XPS)对材料的表面结构及组成进行分析;利用扫描电子显微镜(SEM)及扫描探针显微镜(SPM)观察了材料的形貌;最后对复合材料的力学性能进行了研究。
【Abstract】 In this work,the poly(D,L-Lactic acid)/chondroitin sulfate/chitosan(PDLLA/CS/CHS) composite materials are successfully prepared using the electrostatic self-assembly and vacuum freeze-drying techniques.The self-assembly process is monitored by UV-Vis spectra,while the morphology,as well as the surface structure and composition of the-prepared composite materials are characterized by the scan electron microscopy(SEM) and scan probe microscopy(SPM),Fourier transform infrared spectrophotometer(FT-IR) and X-ray photoelectron spectroscopy(XPS),respectively.Furthermore,the mechanical property of the prepared composite materials is also researched.
【Key words】 composite material; electrostatic self-assembly; vacuum freeze-drying;
- 【文献出处】 武汉理工大学学报 ,Journal of Wuhan University of Technology , 编辑部邮箱 ,2009年10期
- 【分类号】R318.08
- 【被引频次】1
- 【下载频次】257