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仙人掌超微粉挥发性成分研究

Determination of Chemical Constituents of the Volatile Oil from Opuntia dillenii(Ker-Gaw.) Haw

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【作者】 汪凯莎丁丽娜刘建华高玉琼安立群廖川

【Author】 WANG Kai-sha1,2,DING Li-na1,2,LIU Jian-hua2,GAO Yu-qiong2*,AN Li-qun1,2,LIAO Chuan1,2(1.Guizhou University,Guiyang 550025;2.Guizhou Institute of Biotechnology Research and Development,Guiyang 550002,China)

【机构】 贵州大学贵州省生物技术研究开发基地

【摘要】 目的:研究仙人掌中的挥发性成分。方法:利用水蒸气蒸馏法提取经超微粉碎后的仙人掌[Opuntia dillenii(Ker-Gaw.)Haw]挥发油,用GC-MS进行测定,结合计算机检索技术对分离的化合物进行结构鉴定,应用色谱峰面积归一化法计算各成分的相对百分含量。结果:共分离鉴定出32个化学成分,占总成分的98.097%,其中相对百分含量大于2%的分别确定为异丁基邻苯二甲酸酯(Isobutyl phthalate)27.492%,棕榈酸(Palmitic acid)16.716%,丁基邻苯二甲酸酯(Butyl phthalate)11.257%,薄荷脑(Menthol)6.722%,亚油酸(Linoleic acid)5.995%,壬醛(Nonanal)4.594%,乙醛(Hexanal)3.614%,十二酸(Dodecanic acid)3.244%。结论:通过对仙人掌超微粉挥发性成分的分析鉴定及相对含量测定,为综合利用仙人掌植物资源等提供科学依据。

【Abstract】 Objective: To study the chemical constituents of the volatile oil from Opuntia dillenii(Ker-Gaw.) Haw.Method: The chemical compositions of the volatile oil of the plants which were obtained by steam distillation with hexane were analyzed by GC-MS.The constituents were identified by their mass spectra.The relative percentage of the oil constituents was calculated from the GC peak areas.Result: Thirteen-two kinds of chemical constituents in Opuntia dillenii(Ker-Gaw.) Haw were separated and characterized;which were representing 98.097% of the oil.Relative contents that were more than 2% were determined as Isobutyl phthalate 27.492%,Palmitic acid 16.716%,Butyl phthalate 11.257%,Menthol 6.722%,Linoleic acid 5.995%,Nonanal 4.594%,Hexanal 3.614%,Dodecanic acid 3.244%.Conclusion: The composition of volatile oils of micro-milling of Opuntia dillenii(Ker-Gaw.) Haw’s comprehensive utilization to provide reference data.

【基金】 贵州省优秀科技教育人才省长专项资金项目[黔省专合字(2006)81号]资助
  • 【分类号】R284.1
  • 【被引频次】4
  • 【下载频次】154
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