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牛大力藤叶脂溶性成分的GC-MS分析

Analysis of Liposoluble Components of the Leaves from Millettia speciosa by GC-MS

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【作者】 赖富丽王祝年王建荣晏小霞

【Author】 Lai Fuli, Wang Zhunian, Wang Jianrong, Yan Xiaoxia Institute of Tropic Crops Genetic Resources, Chinese Academy of Tropical Agricultural Sciences/ Ministry of Agriculture Key Laboratory for Tropical Crops Germplasm Resources Utilization, Danzhou, Hainan 571737

【机构】 中国热带农业科学院热带作物品种资源研究所农业部热带作物种质资源利用重点开放实验室

【摘要】 采用气相色谱-质谱联用技术(GC-MS)对牛大力藤叶片脂溶性成分进行分析测定,并结合计算机检索技术对其成分进行结构鉴定,应用色谱峰面积归一化法计算各成分的相对百分含量。结果显示,共鉴定了41个化学成分(除豆甾醇外,其余40个化学成分在该植物中属首次报道),其相对含量为81.22%。其中含量较高的成分依次为维生素E(11.52%)、亚麻酸乙酯(10.26%)、γ-谷甾醇(8.53%)、棕榈酸乙酯(8.23%)、叶绿醇(7.00%)、亚麻酸甲酯(5.04%)、亚油酸乙酯(4.13%)、亚油酸(4.09%)和植二烯(3.89%)。

【Abstract】 Chemical constituents of the liposoluble fraction of the leaves from Millettia speciosa Champ. were analyzed by using the gas chromatography-mass spectrometry (GC-MC), and identified by their mass spectra, and their relative percentage was calculated from the GC peak areas. Forty-one compounds were identified, accounting for 81.22% of the total detected constituents. The major constituents identified include Vitamin E (11.52%), ethyl linolenate (10.26%), clionasterol (8.53%), ethyl palmitate (8.23), phytol (7.00%), methyl linolenate (5.04%), ethyl linoleate(4.13%), linoleic acid(4.09%), phytadiene(3.89%), etc. Of all the constituents 40 liposoluble components except stigmasterol were first reported in the leaves of M. speciosa Champ.

【基金】 农业部热带作物资源保护项目(No.RZY-03-2008);中国热带农业科学院品种资源研究所研究生基金项目“牛大力的生物活性成分研究”(No.YJS-2008-S021)资助
  • 【文献出处】 热带作物学报 ,Chinese Journal of Tropical Crops , 编辑部邮箱 ,2009年05期
  • 【分类号】R284.1
  • 【被引频次】38
  • 【下载频次】526
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