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愈创木酚和乙醛酸缩合反应的影响因素
On the Influence Factors of Condensation Reaction by Guaiacol and Glyoxylic Acid
【摘要】 以愈创木酚和乙醛酸为原料-,通过缩合反应试验合成3-甲氧基-4-羟基-苯乙醇酸(MHMA)。研究了原料的配比、原料的加入方式、反应温度、反应时间、反应体系碱浓度等因素对愈创木酚和乙醛酸缩合反应的影响。乙醛酸转化率可达84.0%,MHMA收率可达80%以上。
【Abstract】 Based on condensation of guaiacol and glyoxylic acid,3-methoxy 4-hydroxyman-delic acid(MHMA)was synthesized.Influence factors are investigated on the condensation reaction,the formula of materia,the method of feeding in materia,the reaction temperature,the reaction time,the concentration of alkali of reaction.The rate of conversion(glyoxalic acid)mounts to 84.0 % and the yield of MHMA mounts to 80 %.
【关键词】 愈创木酚;
乙醛酸;
缩合反应;
影响因素;
【Key words】 guaiacol; glyoxylic acid; condensation reaction; influence factors;
【Key words】 guaiacol; glyoxylic acid; condensation reaction; influence factors;
- 【文献出处】 萍乡高等专科学校学报 ,Journal of Pingxiang College , 编辑部邮箱 ,2009年03期
- 【分类号】O621.2
- 【被引频次】1
- 【下载频次】193