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N-苯基氨基邻苯二甲酰亚胺衍生物的合成及初步杀虫活性

Synthesis and Preliminary Bioassay of N-Phenylaminophthalimide Derivatives

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【Author】 LIU Ming1,CUI Yong-liang1,WANG Yi1,DUAN You-sheng1RUI Chang-hui2,WANG Min1,LIU Shang-zhong1(1.Department of Applied Chemistry,China Agricultural University,Key Laboratory of Pesticide Chemistry and Application,Beijing 100193,China;2.Institute of Plant Protection,China Academic of Agricultural Sciences,Beijing 100193,China)

【机构】中国农业大学应用化学系农业部农药化学与应用技术重点开放实验室；中国农业科学院植物保护研究所；

【摘要】为寻找新型环境友好型杀虫剂,用取代苯酐与取代苯肼在冰乙酸中缩合,合成了11个未见杀虫活性报道的N-苯基氨基邻苯二甲酰亚胺衍生物,其中7个是新化合物。所有化合物结构均通过核磁共振氢谱及液质联机(LC-MSD)确认,并利用X-ray单晶衍射确认了A02的晶体结构。初步的杀虫活性测试结果表明,大部分化合物对小菜蛾具有一定的杀虫活性,其中化合物A06在600g/mL下96h的致死率达到84%。更多还原

【Abstract】 In order to discover novel environmental friendly insecticide,11 no insecticidal activity reported N-phenylaminophthalimide derivatives were synthesized through condensation reaction of substituted phthalic anhydride and substituted phenylhydrazine in glacial acetic acid,and 7 among them were new compounds.The structures of all compounds were confirmed with 1H NMR & LC-MSD,and the crystal structure of A02 was characterized by X-ray crystal diffraction method.The preliminary bioassay showed that some compounds had certain insecticidal activity against Plutella xylostella Linnaeus at 600 μg/mL,and the lethal rate of compound A06 was 84% after 96 hours.更多还原

【关键词】 N-苯基氨基邻苯二甲酰亚胺；合成；杀虫活性；
【Key words】 N-phenylaminophthalimide derivatives； synthesis； biological activity；

【基金】国家自然科学基金(20572129);国家“十一五”科技支撑计划基金(2006BAE01A01-11)

【文献出处】农药学学报 ,Chinese Journal of Pesticide Science , 编辑部邮箱 ,2009年01期

【分类号】S482.3
【被引频次】2
【下载频次】282

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