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Synthesis and Crystal Structure Analysis of 2-(3,5-Di-tert-butyl-2-hydroxyphenyl)-2-(3,4- dimethylphenyl) Acetic Acid Dimethylamine Salt

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【Author】 CHENG Jiea, b CHENG Chang-Meib② HE Juana② SHANG Pei-Huab WANG Ru-Jib ZHAO Yu-Fenb a (School of Chemistry and Chemical Engineering, Henan University of Technology, Henan 450052, China) b (Key Laboratory of Bioorganic Phosphorus Chemistry and Chemical Biology, Ministry of Education, Department of Chemistry, School of Life Sciences and Engineering, Tsinghua University, Beijing 100084, China)

【机构】 School of Chemistry and Chemical Engineering, Henan University of Technology； Key Laboratory of Bioorganic Phosphorus Chemistry and Chemical Biology, Ministry of Education, Department of Chemistry, School of Life Sciences and Engineering, Tsinghua University；

【摘要】 A new compound 2-(3,5-di-tert-butyl-2-hydroxyphenyl)-2-(3,4-dimethylphenyl) acetic acid dimethylamine salt ([NH2(CH3)2][C24H31O3]) was synthesized and structurally de- termined. It is of monoclinic system, space group P21/c with a = 14.731(2), b = 10.1185(10), c = 17.065(2) , β = 98.293(10)°, Z = 4, V = 2517.0(6) 3, Dc = 1.091 g/cm3, F(000) = 904 and Mr = 413.58. The dihedral angle defined by two benzene rings is 98.23°.更多还原

【Abstract】 A new compound 2-(3,5-di-tert-butyl-2-hydroxyphenyl)-2-(3,4-dimethylphenyl) acetic acid dimethylamine salt ([NH2(CH3)2][C24H31O3]) was synthesized and structurally de- termined. It is of monoclinic system, space group P21/c with a = 14.731(2), b = 10.1185(10), c = 17.065(2) , β = 98.293(10)°, Z = 4, V = 2517.0(6) 3, Dc = 1.091 g/cm3, F(000) = 904 and Mr = 413.58. The dihedral angle defined by two benzene rings is 98.23°.更多还原

【关键词】 2-(3； 5-di-tert-butyl-2-hydroxyphenyl)-2-(3； 4-dimethylphenyl) acetic acid dimethylamine salt； synthesis； X-ray diffraction； crystal structure；
【Key words】 2-(3； 5-di-tert-butyl-2-hydroxyphenyl)-2-(3； 4-dimethylphenyl) acetic acid dimethylamine salt； synthesis； X-ray diffraction； crystal structure；

【基金】 supported by the Technology Risk Innovation Fund of PetroChina Company Ltd.

【文献出处】结构化学 ,Chinese Journal of Structural Chemistry , 编辑部邮箱 ,2009年04期

【分类号】O621.2
【下载频次】61

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