节点文献
1-硝基萘的简单有效合成
Simple and Efficient Synthesis of 1-Nitronaphthalene
【摘要】 1-硝基萘是合成医药、染料、农药、橡胶防老剂等的重要中间体.报道了一种合成1-硝基萘的简单有效的方法:以单一硝酸(65%~68%)替代传统的由浓硝酸和浓硫酸组成的混酸为硝化剂,在温和条件下方便地制备出1-硝基萘,产率可达86.6%.
【Abstract】 1-nitronaphthalene is an important intermediate for the synthesis of medicines,dyes,agricultural chemicals and rubber antioxidants.In this paper,a simple and effective method for the synthesis of 1-nitronaphthalene is reported.With sole nitric acid(65%~68%) instead of miscible liquids of concentrated sulfuric acid and nitric acid as nitrating agent,1-nitronaphthalene has been produced expediently in yield of 86.6% under mild conditions.
【基金】 河南师范大学青年基金;河南师范大学博士科研启动费支持课题
- 【文献出处】 河南师范大学学报(自然科学版) ,Journal of Henan Normal University(Natural Science) , 编辑部邮箱 ,2009年05期
- 【分类号】TQ246.3
- 【被引频次】6
- 【下载频次】423