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气相色谱法测定土壤中五氯酚
Determination of Pentachlorophenol in Soil by Gas Chromatography
【摘要】 采用索氏提取-气相色谱法测定土壤中的五氯酚,优化了试验条件。方法在0μg/kg~200μg/kg范围内线性良好,检出限为0.03μg/kg,空白土壤加标样测定的RSD为2.6%,回收率为95.4%~101%。
【Abstract】 The pentachlorophenol in soils was determined by GC with Soxhlet extraction.The experimental conditions were optimized to produce the following results: good linearity in the range from 0 μg/kg to 200 μg/kg,the detection limits 0.03 μg/kg,the RSDs of the blank soils added standard samples 2.6%,and the recoveries from 95.4% to 101%.
【关键词】 五氯酚;
索氏提取;
气相色谱法;
土壤;
【Key words】 Pentachlorophenol; Soxhlet extraction; Gas chromatography; Soil;
【Key words】 Pentachlorophenol; Soxhlet extraction; Gas chromatography; Soil;
【基金】 山东省科学院发展基金资助项目(2008-04)
- 【文献出处】 环境监测管理与技术 ,The Administration and Technique of Environmental Monitoring , 编辑部邮箱 ,2009年03期
- 【分类号】X833
- 【被引频次】9
- 【下载频次】243