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多介质环境样品中有机氯农药及其手性成分的分析方法

DETERMINATION METHOD OF ORGANOCHLORINE PESTICIDES AND THEIR CHRIAL COMPONENTS IN ENVIRONMENTAL SAMPLES

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【作者】 王伟李兴红陆海王喜智王晓飞于惠杰徐晓白蒋湘宁

【Author】 WANG Wei 1,2LI Xing-hong1LU Hai2WANG Xi-zhi1,2WANG Xiao-fei1YU Hui-jie3XU Xiao-bai1JIANG Xiang-ning2(1State Key Laboratory of Environmental Chemistry and Ecotoxicology,Research Center of Eco-Environment Sciences,Chinese Academy of Sciences,Beijing,100085,China;2Beijing Forestry University,Beijing,100083,China; 3Beijing Second Artillery General Hospital Center Laboratory,Beijing,100088,China)

【机构】 中国科学院生态环境研究中心环境化学与生态毒理学国家重点实验室北京林业大学北京第二炮兵总医院中心实验室

【摘要】 建立了利用自装填的硫酸硅胶层析柱和商品化固相萃取(SPE)硅胶小柱净化,结合非手性气相色谱和手性气相色谱柱对多介质环境样品中有机氯农药及其手性成分的分析方法.在优化的条件下,对土壤、浮尘、植物(松针)和动物(蚯蚓)样品中有机氯农药及其手性成分进行了分离检测,获得的数据能够为确认环境样品中有机氯农药的来源提供非常有用的信息.

【Abstract】 This paper developed an analytical method to determinate the organochlorine pesticides as well as their chrial components using no-chiral/chiral gas chromatogram column.The cleanup procedures of samples were done through sulfuric acid silica gel and solid phase extraction silica column.Under optimized conditions,target components in soil,dust,needle and earth worm were determined effectively.It was helpful of this method for obtaining data which provided some information to identify/track the source of pollutants in the environment.

【关键词】 有机氯农药土壤浮尘松针蚯蚓
【Key words】 organochlorine pesticidessoildastneedleearth worm.
【基金】 国家自然科学基金(No.20607026)项目
  • 【文献出处】 环境化学 ,Environmental Chemistry , 编辑部邮箱 ,2009年02期
  • 【分类号】X132
  • 【被引频次】4
  • 【下载频次】477
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