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分子蒸馏技术浓缩合成维生素E
Concentration of the synthetical Vitamin E by molecular distillation
【摘要】 对分子蒸馏浓缩合成维生素E进行了研究,在刮膜器转速200r/min、操作压力0.1Pa、蒸馏温度158℃、进料速率110mL/h下,经分子蒸馏处理后的合成维生素E纯度可达到98%以上;同时研究了主要的操作参数对产品纯度的影响;另外,根据实验数据进行拟合,得到了在一定范围内准确度较高的馏出物轻组分浓度预测式。
【Abstract】 The concentration of synthetic vitamin E by molecular distillation was studied.The experimental results showed that the product purity was above 98% under the conditions:wiper speed 200 r/min,operation pressure 0.1Pa,distillation temperature 158°C,feed rate 110 mL/h,and the main operation parameters were studied.In addition,the experimental data were fitted to obtain the concentration predicor equation of the more volatile component.
【关键词】 分子蒸馏;
合成维生素E;
浓度预测式;
【Key words】 molecular distillation; synthetical vitamin E; concentration predict or formula;
【Key words】 molecular distillation; synthetical vitamin E; concentration predict or formula;
【基金】 国家自然科学基金(20576088)资助项目
- 【文献出处】 化工进展 ,Chemical Industry and Engineering Progress , 编辑部邮箱 ,2009年03期
- 【分类号】TQ466.5
- 【被引频次】10
- 【下载频次】602