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牙用纳米ZrO2-白榴石复合烤瓷的制备及性能研究

PREPARATION AND PROPERTIES OF NANO-ZIRCONIA-LEUCITE COMPOSITE PORCELAIN

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【作者】 康明尹光福廖晓明尹星陈坤刘军

【Author】 KANG Ming~(1,2) YIN Guangfu~1 LIAO Xiaoming~1 YIN Xing~3 CHEN Kun~2 LIU Jun~2(1.College of Materials Science and Engineering,Sichuan University,Chengdu 610065;2.College of Material Science and Engineering,Southwest University of Science and Technology,Mianyang 621010,Siehuan;3.West China College of Stomatology,Sichuan University,Chengdu 610041,China)

【机构】 四川大学材料科学与工程学院西南科技大学材料科学与工程学院四川大学华西口腔医学院

【摘要】 以钾长石、碳酸钾和纳米氧化锆为主要原料,通过高温同相法,一次性合成了一种牙用白榴石-氧化锆复合烤瓷粉。利用X射线衍射仪和扫描电镜分析烤瓷材料的物相结构,利用万能试验机和热膨胀仪分别测试样品的弯曲强度和热膨胀系数。结果表明:纳米氧化锆的加入,既有利于烤瓷材料的弯曲强度的提高,又有助于调节烤瓷材料的热膨胀系数。当氧化锆的添加量为8%(质量分数),合成烤瓷粉的煅烧温度为1200℃.熔附温度为900℃时,样品的弯曲强度为112MPa,热膨胀系数为14.4×10-6/K。

【Abstract】 The dental zirconia-leucite composite porcelain powder was synthesized by the solid-state method using nano-zirconia and potassium carbonate as raw materials.X-ray diffraction and scanning electron microscopy were employed to characterize the phase structure of the porcelain material.The bending strength and the thermal expansion coefficient of the samples were measured by uni- versal testing machine and thermal expansion instrument,respectively.The results show that the addition of nano-zirconia is favorable not only for increasing the bending strength of the porcelain material but also for controlling their thermal expansion coefficient.With 8% ZrO2,the sintering temperature of 1200℃and the fusing temperature of 900℃,the bending strength and the thermal expansion coefficient of the prepared sample are 112 MPa and 14.4×10-6/K,respectively.These results suggest that it will have promising clinical applications in dental restoration.

【关键词】 钾长石氧化锆白榴石烤瓷粉
【Key words】 potash feldsparzirconialeuciteporcelain powder
【基金】 国家自然科学基金(10476024);四川省教育厅项目(06zd1108)资助。
  • 【文献出处】 硅酸盐学报 ,Journal of the Chinese Ceramic Society , 编辑部邮箱 ,2009年01期
  • 【分类号】TQ174.759
  • 【被引频次】7
  • 【下载频次】252
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