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Synthesis and microstructure analysis of composite Nd:YAG/YAG transparent ceramics

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【作者】 姜本学黄同德吴玉松刘文斌潘裕柏

【Author】 Benxue Jiang,Tongde Huang,Yusong Wu,Wenbin Liu,and Yubai Pan Shanghai Institute of Ceramics,Chinese Academy of Sciences,Shanghai 200050,China

【机构】 Shanghai Institute of Ceramics,Chinese Academy of Sciences

【摘要】 Transparent Nd:YAG/YAG composite ceramics are synthesized by solid-state reaction method using highpurity Y2O3,Al2 O 3,and Nd2O3 powders as raw materials.The mixed powder compacts are sintered at 1780°C for 10 h under vacuum and annealed at 1450°C for20 h in air.The Nd:YAG/YAG ceramics exhibit a pore free structure with an average grain size of about 30 μm.The microstructure of the Nd:YAG/YAG composite transparent ceramics is studied and there is no interface between Nd:YAG and YAG ceramics.The Nd ion distribution in one grain is also studied,which shows that there is no segregation of Nd ions as in Nd:YAG crystals.

【Abstract】 Transparent Nd:YAG/YAG composite ceramics are synthesized by solid-state reaction method using highpurity Y2O3,Al2 O 3,and Nd2O3 powders as raw materials.The mixed powder compacts are sintered at 1780°C for 10 h under vacuum and annealed at 1450°C for20 h in air.The Nd:YAG/YAG ceramics exhibit a pore free structure with an average grain size of about 30 μm.The microstructure of the Nd:YAG/YAG composite transparent ceramics is studied and there is no interface between Nd:YAG and YAG ceramics.The Nd ion distribution in one grain is also studied,which shows that there is no segregation of Nd ions as in Nd:YAG crystals.

【基金】 supported by the 42nd China Postdoctoral Science Foundation;the Applied Basic Research Program of Sciences and Technology Commission Foundation of Shanghai (No.06DZ11417);the National “863” Program of China (No.2007AA03Z523)
  • 【文献出处】 Chinese Optics Letters ,中国光学快报(英文版) , 编辑部邮箱 ,2009年06期
  • 【分类号】TN244
  • 【被引频次】3
  • 【下载频次】99
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