【摘要】 采用原位合成法,使用壬基酚聚氧乙烯醚(Tx-15)和脂肪醇聚氧乙烯醚(AEO-9)做为模板剂,在中性条件下合成W-MSU-1和W-MSU-2介孔分子筛,合成中使用乙酰丙酮(HAcac)作为助剂,考察其对介孔结构的影响,通过X射线衍射仪(XRD)、傅里叶红外光谱仪(FT-IR)、扫描电镜(SEM)、低温N2吸附对样品进行表征.结果表明,加入过渡金属氧化物有助于介孔的形成,助剂的使用提高了孔的结构参数.更多还原

【Abstract】 The polyoxyethylene nonylphenolether(Tx-15)and fattyalcohol polyoxyethylene ether(AEO-9) are used as templates in neutral condition for in-situ synthesis W-MSU-1,W-MSU-2 mesoporous molecular zeolites.Acetylacetone as additional reagent is used.The structure characterization is demonstrated by XRD,FT-IR,SEM,N2 adsorption.The results show that,the transitional metal oxide conduce to form the mesoporous,the reagent can modify the structure parameter.更多还原