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Cu2O-Cu复合材料制备工艺的研究
Study on Preparation of Cu2O-Cu Composites
【摘要】 以Cu2O和炭黑粉末为原料,采用原位还原-无压(热压)烧结工艺制备Cu2O-Cu复合材料。利用XRD和OM对烧结试样进行研究,并测试其力学性能。研究表明,复合材料由Cu和Cu2O两相组成,原位还原-无压烧结法的合理烧结时间为5h,其力学性能高于传统粉末冶金法制备复合材料力学性能,抗压强度464MPa。原位还原-热压烧结法可以改善试样致密性及细化微观组织,进一步提高力学性能,抗压强度达到702MPa。
【Abstract】 Cu-Cu2O composites were prepared from C and Cu2O powders,called as in-situ reduction-pressure less sintering (IRPS) method and in-situ reduction-hot pressing (IRHP) method. Samples were characterized by X-ray diffraction and optical microscope. XRD analysis shows that the samples only consist of Cu2O and Cu phases. The microstructure analysis shows that the optimum sintering time for the IRPS method is 5 h at 1050 ℃,and the IRHP method leads to lower porosity and smaller Cu2O matrix crystal sizes. The compressive strength of the sample prepared by IRPS method is higher than thoseprepared by conventional powder metallurgic method (PMM). The compressive strength of the sample prepared by IRHP method is higher than those prepared by IRPS method.
【Key words】 Cu-Cu2O composites; in-situ reduction; microstructure; compressive strength;
- 【文献出处】 稀有金属材料与工程 ,Rare Metal Materials and Engineering , 编辑部邮箱 ,2009年S2期
- 【分类号】TB332
- 【下载频次】143