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块体多孔金属镍的逐层扫描喷射电沉积制备

Research on Technological Process of Bulk Porous Nickel Prepared by Scanning Jet Electrodeposits

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【作者】 宫凯黄因慧田宗军刘志东王桂峰

【Author】 GONG Kai,HUANG Yin-hui,TIAN Zong-jun,LIU Zhi-dong,Wang Gui-feng(Jiangsu Key Laboratory of Precision and Micro-Manufacturing Technology,Nanjing University of Aeronautics and Astronautics,Naijing 210016,China)

【机构】 南京航空航天大学江苏省精密与微细制造技术重点实验室

【摘要】 介绍了基于喷射电沉积的逐层扫描法制备块状多孔金属镍的原理,利用该工艺在自行研制的试验装置上制备块状多孔金属镍。利用电子扫描显微镜(SEM)对多孔金属镍块状试样的表面形貌、微观组织结构及孔隙率进行检测,对表面显微硬度和压缩性能进行测试。结果表明:多孔金属镍样品的多孔层由向上生长的枝状晶围成三维连通孔隙,通孔分布均匀致密。经SEM分析铸层表面,可见枝状晶分支由菜花状的晶胞叠加生长形成。使用加工电流密度为900 A/dm2时,制备的块状样品孔隙率为61.5%。表面的显微硬度HV为330.5。压缩性能的检测结果表明,多孔金属的抗压屈服极限为11.85MPa。应力曲线存在一个很宽的塑性平台,具有典型的塑性多孔材料特征。

【Abstract】 The bulk porous nickel sample was introduced and made by jet scanning electrodeposition forming.The surface morphology,microstructure,grain size of the micro-cell structure of deposition,were studied and analyzed by means of SEM,and the mechanical properties of the sample were also studied,such as surface micro-hardness and compressive property.The results show that,using jet scanning electrodeposition in current density of 900A/dm2,the prepared sample’s porosity is 61.5%.The surface micro-hardness of the sample reaches to HV 330.5.The compressive yield stress of porous nickel is 11.85MPa,which has a large number of plastic deformations of the absorption capacity.

【基金】 国家自然科学基金资助项目(50575104)
  • 【文献出处】 材料工程 ,Journal of Materials Engineering , 编辑部邮箱 ,2009年08期
  • 【分类号】TG146.15
  • 【被引频次】3
  • 【下载频次】185
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