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块体多孔金属镍的逐层扫描喷射电沉积制备
Research on Technological Process of Bulk Porous Nickel Prepared by Scanning Jet Electrodeposits
【摘要】 介绍了基于喷射电沉积的逐层扫描法制备块状多孔金属镍的原理,利用该工艺在自行研制的试验装置上制备块状多孔金属镍。利用电子扫描显微镜(SEM)对多孔金属镍块状试样的表面形貌、微观组织结构及孔隙率进行检测,对表面显微硬度和压缩性能进行测试。结果表明:多孔金属镍样品的多孔层由向上生长的枝状晶围成三维连通孔隙,通孔分布均匀致密。经SEM分析铸层表面,可见枝状晶分支由菜花状的晶胞叠加生长形成。使用加工电流密度为900 A/dm2时,制备的块状样品孔隙率为61.5%。表面的显微硬度HV为330.5。压缩性能的检测结果表明,多孔金属的抗压屈服极限为11.85MPa。应力曲线存在一个很宽的塑性平台,具有典型的塑性多孔材料特征。
【Abstract】 The bulk porous nickel sample was introduced and made by jet scanning electrodeposition forming.The surface morphology,microstructure,grain size of the micro-cell structure of deposition,were studied and analyzed by means of SEM,and the mechanical properties of the sample were also studied,such as surface micro-hardness and compressive property.The results show that,using jet scanning electrodeposition in current density of 900A/dm2,the prepared sample’s porosity is 61.5%.The surface micro-hardness of the sample reaches to HV 330.5.The compressive yield stress of porous nickel is 11.85MPa,which has a large number of plastic deformations of the absorption capacity.
【Key words】 porous metal; dendritic crystal; jet electrodeposition; microhardness; compressive property;
- 【文献出处】 材料工程 ,Journal of Materials Engineering , 编辑部邮箱 ,2009年08期
- 【分类号】TG146.15
- 【被引频次】3
- 【下载频次】185