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GC-MS法鉴别藿香正气丸中广藿香和厚朴
GC-MS Identification of Pogostemon cabin and Cortex Magnoliae Officinalis in Huoxiang Zhengqi Pills
【摘要】 目的:采用气相色谱-质谱联用(GC-MS)法鉴别藿香正气丸中的广藿香和厚朴。方法:采用超声萃取技术提取藿香正气丸的成分,色谱柱为SPB-1701石英毛细柱(30m×0.25mm×0.25μm),载气为He,离子源为EI源,电子能量为70eV。结果:可同时鉴别出来自广藿香的广藿香醇和来自厚朴的厚朴酚、和厚朴酚等主要成分。结论:该方法简便、迅速、准确、可靠,可用于藿香正气丸的质量控制。
【Abstract】 OBJECTIVE: To identify Pogostemon cablin and Cortex Magnoliae Officinalis in Huoxiang zhengqi pills by Gas Chromatography-Mass Spectrometry. METHODS:Pogostemon cablin and Cortex Magnoliae Officinalis in Huoxiang zhengqi pills were extracted by ultrasound extraction technology and identified on SPB-1701 column(30 m×0.25 mm×0.25 μm) with He as carrier gas and EI as ion source at an electron energy of 70 eV. RESULT:The main components such as Patchouli alcohol from Pogostemon cablin,and Magnolol and Honokiol from Cortex Magnoliae Officinalis were identified simultaneouly. CONCLUSION: The method is simple,rapid,accurate and reliable,and applicable for the quality control of Huoxiang zhengqi pills.
【Key words】 Gas chromatography-mass spectrometry; Huoxiang zhengqi pills; Pogostemon cablin; Cortex Magnoliae Officinalis; Identification;
- 【文献出处】 中国药房 ,China Pharmacy , 编辑部邮箱 ,2008年36期
- 【分类号】R286
- 【被引频次】2
- 【下载频次】272