节点文献
高效液相色谱法测定消肿活血合剂中芍药苷含量
Determination of Paeoniflorin in Xiaozhong Huoxue Mixture by HPLC
【摘要】 目的建立消肿活血合剂中芍药苷的含量测定方法。方法采用高效液相色谱(HPLC)法测定消肿活血合剂中芍药苷的含量。结果芍药苷进样量在0.1001~2.002μg范围内呈良好的线性关系,r=0.9998(n=5),平均加样回收率为99.52%,RSD=0.67%(n=9)。结论该法操作简便,结果准确、可靠,重现性好,可用于消肿活血合剂的质量控制。
【Abstract】 Objective To establish a method for the determination of paeoniflorin in Xiaozhong Huoxue Mixture.Methods The content of paeoniflorin was determined by HPLC.Results The linear range was 0.100 1- 2.002 μ g and the average recovery rate was 99.52% ,RSD=0.67% (n=9).Conclusion The method is simple,reliable and accurate with good reproducibility,which can be used to control the quality of Xiaozhong Huoxue Mixture.
【关键词】 消肿活血合剂;
高效液相色谱法;
芍药苷;
含量测定;
【Key words】 Xiaozhong Huoxue Mixture; HPLC; paeoniflorin; content determination;
【Key words】 Xiaozhong Huoxue Mixture; HPLC; paeoniflorin; content determination;
- 【文献出处】 中国药业 ,China Pharmaceuticals , 编辑部邮箱 ,2008年23期
- 【分类号】R286
- 【被引频次】2
- 【下载频次】24