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中草药制剂的回收乙醇中杂质的去除方法探讨

Study on the removal of impurities in recycled ethanol of medicinal herb preparations

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【作者】 蒋三元曾志坚林传辉罗浩章梁永广

【Author】 JIANG San-yuan~1 ZENG Zhi-jian~2 LIN Chuan-hui~3 LUO Hao-zhang~2 LIANG Yong-guang~1 (1.Xinhui Hospital of Traditional Chinese Medicine,Jiangmen 529100,China;2.Jiangmen Institute for Drug Control,Jiangmen 529000,China;3.Siqianzhen Hospital of Xinhui Jiangmen Guangdong,Jiangmen 529159,China)

【机构】 广东省江门市新会区中医院广东省江门市药品检验所广东省江门市新会区司前镇卫生院广东省江门市新会区中医院 广东江门 529100广东江门 529000广东江门 529159广东江门 529100

【摘要】 目的:探讨中草药制剂的回收乙醇中杂质的去除方法。方法:将回收乙醇进行初步的除杂质实验,选择较好的除杂质方法,再以正交法对其进行优选,并对优选方法加以验证。结果:每1 000 ml回收乙醇中加入5%高锰酸钾溶液6 ml,静置30 min,然后加入活性炭6 g,再静置30 min,滤过,蒸馏,收集蒸馏液作相应的检验,各项指标均能达到规定要求。结论:该方法可有效除去中草药制剂回收乙醇中的杂质,提高其质量。

【Abstract】 Objective:To discuss the method about how to remove the impurities in recycled ethanol of medicinal herb preparations.Methods:The initial test was carried out to remove the impurities in recycled ethanol and the better method was chosen which would be verified by orthogonal test.Results:1 000 ml of recycled ethanol liquor solution was put in 6 ml of 5%KMNO4,standing for 30 min and 6 g of activated carbon,standing for 30 min again.Then it was filtrated and dis- tilled,and the distilled ethanol was collected to make corresponding tests.All indexes of ethanol tests had reached regu- lary request.Conclusion:This method can remove the impurities in recycled ethanol of medicinal herb preparations.The quality of recycled ethanol is improved.

  • 【文献出处】 中国医药导报 ,China Medical Herald , 编辑部邮箱 ,2008年05期
  • 【分类号】TQ461
  • 【被引频次】5
  • 【下载频次】338
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