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大孔吸附树脂吸附分离丰城鸡血藤总黄酮的研究

Adsorption and Separation of Total Flavones from Millettla nitida var. hirsutissima by Macroporous Adsorption Resin

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【作者】 王婷婷曹树稳余燕影万春花

【Author】 WANG Ting-ting1,CAO Shu-wen1,2,YU Yan-ying2,WAN Chun-hua31State Key Laboratory of Food Science and Technology,Nanchang University,Nanchang 330047,China;2Department of Chemistry,Nanchang University,Nanchang 330031,China;3Jiangxi Institute of Analysing and Testing,Nanchang 330029,China

【机构】 南昌大学食品科学与技术国家重点实验室南昌大学化学系江西省分析测试研究所 南昌330047南昌330047 南昌大学化学系南昌330031南昌330029

【摘要】 通过静态吸附实验研究了AB-8和H103两种大孔吸附树脂对丰城鸡血藤总黄酮的吸附特性,筛选出适合丰城鸡血藤总黄酮分离纯化的树脂,并对其进行了动态吸附特性研究。结果表明,AB-8树脂对丰城鸡血藤总黄酮具有良好的吸附和解吸性能,经AB-8树脂吸附富集后,样品总黄酮含量由7.44%提高至40.61%,刺芒柄花素含量提高了15.7倍。因而,AB-8是良好的吸附分离丰城鸡血藤黄酮类化合物的吸附剂。

【Abstract】 The adsorption characteristics of total flavones from M.nitida var.hirsutissima on AB-8 and H103 were investigated by static adsorption experiments.It was found that AB-8 resin had excellent adsorption and desorption capacity to the total flavones.The dynamic adsorption characteristics of the total flovones on AB-8 resin were studied.The content of total flavones of the tested sample increased from 7.44% to 40.61%,the content of formononetin increased by 15.7-fold after the adsorption concentrating on the AB-8 resin.Thus,AB-8 resin was a excellent resin for separating the flavonoids from M.nitida var.hirsutissima.

【基金】 国家自然科学基金(20562008);国家“十一五”科技支撑计划(2006BAI06A18-06);长江学者和创新团队发展计划(IRT0540)
  • 【文献出处】 天然产物研究与开发 ,Natural Product Research and Development , 编辑部邮箱 ,2008年03期
  • 【分类号】R284
  • 【被引频次】15
  • 【下载频次】460
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