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山楂中三萜酸成分的研究
Study on the Triterpene Acids in Fruit of Crataegus pinnatifida
【摘要】 目的研究山楂果的三萜酸类化学成分。方法以制备型高效液相色谱法从山楂果中分离纯化三萜酸类成分,并通过化学方法和波谱分析(IR,MS,1HNMR,13CNMR)进行成分确认。结果共获得4个三萜酸成分,并确定它们的化学结构分别为:山楂酸(Maslinic acid,Ⅰ),科罗索酸(Corosolic acid,Ⅱ),齐墩果酸(oleanlic acid,Ⅲ),熊果酸(ursolic acid,Ⅳ)。结论化合物Ⅱ为首次从该植物中获得。
【Abstract】 Objective To study triterpene acids in the fruit of Crataegus pinnatifida.Methods Four triterpenoidal acids were isolated from the extraction of the fruit of Crataegus pinnatifida by pre-HPLC,which were identified by chemical method and spectroscopic(IR,MS,1HNMR,13CNMR).Results The compounds were identified as: Maslinic acid(Ⅰ),Corosolic acid(Ⅱ),oleanlic acid(Ⅲ),ursolic acid(Ⅳ).Conclusion The compounds corosolic acid is obtained from the fruit of Crataegus pinnatifida for the first time.
【关键词】 山楂果;
三萜酸;
科罗索酸;
【Key words】 The fruit of Crataegus pinnatifida; Triterpene acids; Corosolic acid;
【Key words】 The fruit of Crataegus pinnatifida; Triterpene acids; Corosolic acid;
【基金】 国家星火基金项目(No.2006EA710024);安徽省合肥市2007年度人才发展基金项目
- 【文献出处】 时珍国医国药 ,Lishizhen Medicine and Materia Medica Research , 编辑部邮箱 ,2008年12期
- 【分类号】R284.2
- 【被引频次】73
- 【下载频次】932