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气相色谱-质谱联用法测定中药姜花块根挥发油化学成分

Determination of Chemical Constituents in Volatile Oil from Hedychium coronarium

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【作者】 彭炳先黄振中陈莉莉陈受惠

【Author】 PENG Bing-xian,HUANG Zhen-zhong,CHEN Li-li,CHEN Shou-hui(College of Chemistry and Chemical Engineering,Jiangxi Normal University,Nanchang 330022,China)

【机构】 江西师范大学化学化工学院江西师范大学化学化工学院 江西南昌330022江西南昌330022

【摘要】 目的研究姜花块根挥发油的化学成分。方法采用水蒸气蒸馏法提取姜花块根挥发油,用气相色谱-质谱联用仪对其进行分离测定,结合计算机检索对分离的化合物进行结构鉴定,应用色谱峰面积归一化法测定各成分的相对百分含量。结果水蒸气蒸馏提取物得率为0.12%,分别鉴定出46个化学成分。结论姜花块根挥发油成分主要为萜类及倍半萜衍生物。

【Abstract】 Objective To study the chemical constituents of the volatile oil from Hedychium coronarium roots.Methods The volatile oil was obtained by steam distillation.The chemical constituents were separated and identified by GC-MS.The relative contents in the volatile oil were determined by area normalization.Results The extraction rate of Hedychium coronarium roots was 0.09%,and 46 chemical constituents were separated and identified.Conclusion The main chemical constituents of Hedychium coronarium roots are derivant of terpene and sesquiterpenoids.

【关键词】 姜花挥发油气相色谱-质谱联用
【Key words】 Hedychium coronariumVolatile oilGC-MS
  • 【文献出处】 时珍国医国药 ,Lishizhen Medicine and Materia Medica Research , 编辑部邮箱 ,2008年06期
  • 【分类号】R284
  • 【被引频次】8
  • 【下载频次】277
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