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强酸性大孔树脂催化合成肉桂酸正丙酯的研究
Study on synthesis of n-propyl cinnamate catalysized by strong acidic macroporous resin
【摘要】 应用强酸性大孔树脂CAT600做催化剂合成肉桂酸正丙酯,通过优化合成工艺得到最佳工艺条件:肉桂酸0.02 moL,酸醇摩尔比1∶5,催化剂用量45%,反应时间3.5 h,在此条件下产率达94.30%。
【Abstract】 The n-propyl cinnamate was synthesized with CAT-600 strong acidic macroporous resin as catalyzer.The preparation processes were investigated and optimum conditions were: cinnamate was 0.02 moL,the molar ratio of cinnamate to npropyl alcoho1 was 1∶5,the amount of catalyzer was 45 %,the reactive time was 3.5 h and the yield of the product was 94.30 %.
【关键词】 肉桂酸正丙酯;
合成;
强酸性大孔树脂;
催化;
【Key words】 n-propyl cinnamate; synthesis; strong acidic macroporous resin; catalysis;
【Key words】 n-propyl cinnamate; synthesis; strong acidic macroporous resin; catalysis;
【基金】 广东省自然科学基金资助项目(06023571)
- 【文献出处】 粮油食品科技 ,Science and Technology of Cereals,Oils and Foods , 编辑部邮箱 ,2008年05期
- 【分类号】TQ245.24;TQ655
- 【被引频次】1
- 【下载频次】76