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乙醇水溶液浸出棉籽粕中棉籽糖的实验研究

Studies on Leaching Raffinose From Cottonseed Meal With the Solvent of Ethanol-water

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【作者】 戴卫东汪守建卢伯南钱礼华

【Author】 DAI Wei-dong,WANG Shou-jian,LU Bo-nan,QIAN Li-hua (Department of Chemical Engineering,Huaihai Institute of Technology,Jiangsu Lianyungang 222005,China)

【机构】 淮海工学院化学工程学院

【摘要】 分别考察了不同浓度的乙醇水溶液、浸取温度、浸出时间和料液比的操作工艺条件对棉籽糖浸取率的影响。结果表明,低浓度的乙醇水溶液、较高的温度、较长的浸出时间、较大的料液比有利于棉籽糖的浸出。较佳的操作条件为:乙醇溶液浓度为80%,提取温度为55℃,浸出时间为2.5h,提取料液比为1:12(W/V),棉籽糖的浸出率可达90%以上。

【Abstract】 Raffinose is soluble in water,acetone,ethanol-water solution and other polar soutions.Protein of cottonseed meal is also dissolved.Therefore,ethanol-water solution was chosen as a solvent to leach raffinose of cottonseed meal.The leaching rate of raffinose were investigated under different ethanol concentrations in ethanol-water solution,leaching temperature,extraction time and cottonseed-meal/ sovent ratio.The results showed that lower concentrations of ethanol-water,higher temperature,longer time,larger cottonseed-meal/ solvent ratio comduce to increasing raffinose leaching yield.Better operating conditions was ethanol concentration of 80%, temperature of 55℃ extraction,time of 2.5h extraction,solid-liquid ratio of 1:12.The extraction rate of raffinose was to 90%.

【关键词】 棉籽粕棉籽糖浸出乙醇溶液
【Key words】 Cottonseed mealRaffinoseLeachingEthanol-water solution
【基金】 淮海工学院自然科学基金(Z2004046)
  • 【文献出处】 当代化工 ,Contemporary Chemical Industry , 编辑部邮箱 ,2008年05期
  • 【分类号】TQ914.1
  • 【被引频次】2
  • 【下载频次】135
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