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三氟百菌清的气相色谱分析
Analysis of 5-Chloro-2,4,6-trifuoro-1,3-benzenedicarbonitrile by Gas Chromatography
【摘要】 采用HP-5毛细管色谱柱,以联苯为内标物,用FID检测器对三氟百菌清原药进行定量分析方法研究。进样口温度:240℃,检测器温度:240℃,柱箱温度:170℃,方法的变异系数为0.41%,回收率为98.6%~101.0%。
【Abstract】 A method for the determination of 5-chloro-2,4,6-trifuoro-1,3-benzenedicarbonitrile by GC with HP-5 column using biphenyl as internal standard was developed. Injector temperature was 240 °C, detector temperature was 240 °C, and column temperature was 170 °C. Coefficient of variation for the method was 0.41% and recovery rate was 98.6-101.0%.
- 【文献出处】 农药 ,Agrochemicals , 编辑部邮箱 ,2008年07期
- 【分类号】TQ450.7
- 【下载频次】87