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内标法定量分析α-蒎烯、β-蒎烯、对伞花烃和长叶烯
Quantitative Analysis of α-Pinene,β-Pinene,p-Cymene and Longifolene by Internal Standard Method
【摘要】 选用正十二烷为内标物,采用内标法对α-蒎烯、β-蒎烯、对伞花烃和长叶烯进行了定量分析。确定了最优的气相色谱分析条件,分别测定了α-蒎烯、β-蒎烯、对伞花烃和长叶烯的相对质量校正因子和线性回归相关系数。用内标法和面积归一法分别对试样进行了定量分析,结果表明两者误差小于2.33%。
【Abstract】 A method was introduced for quantitative analysis of α-pinene,β-pinene,p-cymene and longifolene by 1102-Gas Chromatograph with the n-dodecane as internal standard.The optimal conditions for GC analysis were confirmed and the relative mass correction factors and the linear correlation coefficients of α-pinene,β-pinene,pcymene and longifolene were determined.Internal standard method and area nomalization method were used to determine the sample,respectively and the result showed that the relative error was less than 2.33 %.
【基金】 国家自然科学基金资助项目(30560119);广西研究生教育创新计划项目(2006105930817M30);广西青年基金资助项目(0640001);广西自然科学基金资助项目(0575003);广西大学科研基金资助项目(X061020)
- 【文献出处】 生物质化学工程 ,Biomass Chemical Engineering , 编辑部邮箱 ,2008年01期
- 【分类号】TQ651
- 【被引频次】7
- 【下载频次】418