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气相色谱-质谱法分析山黄皮果皮挥发油成分

Analysis of Essential Oil from The Fruit Peel of Clausena indica(Datz.)Oliv by Gas Chromatography-Mass Spectrometry

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【作者】 周红黄克健潘智文黄冠苏涛林翠梧

【Author】 ZHOU Hong1,HUANG Ke-jian2,PAN Zhi-wen1,HUANG Guan1,SU Tao1,LIN Cui-wu1 (1.College of Chemistry and Chemical Engineering,Guangxi University,Nanning 530004,Guangxi,China;2.Institute of Forensic Science,Bureau of Public Security of Guangxi,Nanning 530012,Guangxi,China)

【机构】 广西大学化学化工学院广西壮族自治区公安厅物证鉴定中心广西大学化学化工学院 广西南宁530004广西南宁530012广西南宁530004

【摘要】 用水蒸气蒸馏法提取山黄皮果皮挥发油,经气相色谱-质谱联机分析,共分离出60个峰,鉴定出57种化合物,占总峰面积的99.89%。挥发油主要成分为:β-月桂烯、肉豆蔻醚、异松油烯、3-蒈烯、D-柠檬烯、(+)-2-蒈烯、β-水芹烯、α-水芹烯、石竹烯、丁子香酚甲基醚、(2E)-2,7-二甲基-2,6-辛二烯-1-醇、β-细辛脑,其质量分数分别为:51.50%、24.83%、12.82%、1.94%、1.15%、1.12%、0.55%、0.44%、0.43%、0.42%、0.38%、0.30%。

【Abstract】 The essential oil from the fruit peel of Clausena indica(Datz.)Oliv was extracted by steam distillation and separated by GC.GC-MS exhibited 60 peaks,among which 57 compounds were identified,accounting for 99.89% of the total essential oil.The major constituents of the volatiles are β-myrcene,myristicin,terpinolene,3-carene,D-limonene,(+)-2-carene,β-phellandrene,α-phellandrene,caryophyllene,methyleugenol,(2E)-2,7-dimethyl-2,6-octadien-1-ol and β-asarone,with mass fractions of 51.50%,24.83%,12.82%,1.94%,1.15%,1.12%,0.55%,0.44%,0.43%,0.42%,0.38% and 0.30% respectively.

  • 【分类号】TS207.3;O657.63
  • 【被引频次】7
  • 【下载频次】436
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