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氟化试剂三乙胺三氟化氢的合成研究
Study on synthesis of triethylamine tris(hydrogen fluoride) as fluorinating reagents
【摘要】 三乙胺三氟化氢具有较高的沸点,无腐蚀性,作为氟化试剂广泛应用于有机化合物的电化学选择氟化。以三乙胺和无水氟化氢为原料,四氯化碳为溶剂,合成了标题化合物。
【Abstract】 Triethylamine tris(hydrogen fluoride) is synthesized,using triethylamine and anhydrous hydrogen fluoride as starting materials and carbon tetrachloride as the solvent.It is a reagent with high boiling point and does not have corrosive action to glass ware,and as fluorinating reagents is widely used for electrochemical selective fluorination of organic compounds.
【关键词】 氟化试剂;
三乙胺三氟化氢;
电化学氟化;
合成;
【Key words】 fluorinating reagents; triethylamine tris(hydrogen fluoride); electrochemical selective fluorination; synthesis;
【Key words】 fluorinating reagents; triethylamine tris(hydrogen fluoride); electrochemical selective fluorination; synthesis;
- 【文献出处】 化学试剂 ,Chemical Reagents , 编辑部邮箱 ,2008年10期
- 【分类号】O623.7
- 【被引频次】3
- 【下载频次】649