节点文献
微波辐射无溶剂维生素C催化合成环己酮乙二醇缩酮
Synthesis of Cyclohexanone Ethylene Ketal by Microwave Irradiation Solvent-free Method Catalyzed by Vitamin C
【摘要】 以维生素C为催化剂,采用微波辐射无溶剂催化合成环己酮乙二醇缩酮,探索了不同反应条件对产率的影响。实验结果表明,该方法具有反应时间短(3 min)、产率高(78.8%)、无污染等特点。
【Abstract】 Cyclohexanone ethylene ketal was synthesized using vitamin C as the catalyst by microwave irradiation solvent-free method.The different conditions affected on yield were investigated.The result showed that the reaction time was short(3 min),the yields was high(78.8%) and it had not pollute.
【关键词】 微波辐射;
无溶剂;
维生素C;
环己酮乙二醇缩酮;
【Key words】 microwave irradiation; solvent-free; vitamin C; cyclohexanone ethylene ketal;
【Key words】 microwave irradiation; solvent-free; vitamin C; cyclohexanone ethylene ketal;
【基金】 安徽省滁州学院自然科学研究重点项目,批准号:2006kyz004
- 【文献出处】 化工技术与开发 ,Technology & Development of Chemical Industry , 编辑部邮箱 ,2008年03期
- 【分类号】TQ655
- 【被引频次】6
- 【下载频次】147