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Ni-W合金原位拉伸形变的电子背散射衍射分析
In-situ tensile deformation of Ni-W alloys analyzed by electron backscatter diffraction
【摘要】 采用配置在场发射扫描电镜中的电子背散射衍射仪和应变微拉伸仪,统计分析了Ni-W合金在原位单轴拉伸变形过程中,显微结构、晶界分布、晶粒转动及晶体学取向的变化。在形变(ε=22%)过程中,Ni-9%W合金中的大量晶粒转动,产生滑移,并分为亚晶。应变使大角度晶界的含量增加,挛晶界明显减小,晶粒转动量达15°。立方织构(001)[100]随拉伸形变量的增加而减小。
【Abstract】 The thermal field emission SEM equipped with an electron backscatter diffraction tester and a strain micro-tester was used to statistic analyzing variations in microstructure,grain boundary distribution,lattice orientation rotation and grain orientation of Ni-W alloys during in-situ process of uniaxial tensile deformation.A large number of grains in Ni-9%W alloy rotate during deformation process(ε=22%) are divided into sub-grains due to the multiple slip.Because of the strain,the amounts of the high angle boundary increases,the twin boundary remarkable decreases and the lattice orientation increase of 15° in the Ni-9%W alloy.The cubic texture of(001) decreases with the increase in the tensile deformation.
【Key words】 in-situ deformation; EBSD; misorientation; grain boundary characteristics;
- 【文献出处】 电子显微学报 ,Journal of Chinese Electron Microscopy Society , 编辑部邮箱 ,2008年06期
- 【分类号】TG146.15
- 【下载频次】270