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Ni-W合金原位拉伸形变的电子背散射衍射分析

In-situ tensile deformation of Ni-W alloys analyzed by electron backscatter diffraction

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【作者】 王丽田彦宝张隐奇吉元索红利高忙忙祝永华

【Author】 WANG Li,TIAN Yan-bao,ZHANG Yin-qi,JI Yuan (Beijing University of Technology Institute of Microstructure and Property of Advanced Materials,Beijing 100124)SUO Hong-li,GAO Mang-mang,ZHU Yong-hua (Beijing University of Technology Institute the college of Material Science and Engineering,Beijing 100124)

【机构】 北京工业大学固体微结构与性能研究所北京工业大学材料学院

【摘要】 采用配置在场发射扫描电镜中的电子背散射衍射仪和应变微拉伸仪,统计分析了Ni-W合金在原位单轴拉伸变形过程中,显微结构、晶界分布、晶粒转动及晶体学取向的变化。在形变(ε=22%)过程中,Ni-9%W合金中的大量晶粒转动,产生滑移,并分为亚晶。应变使大角度晶界的含量增加,挛晶界明显减小,晶粒转动量达15°。立方织构(001)[100]随拉伸形变量的增加而减小。

【Abstract】 The thermal field emission SEM equipped with an electron backscatter diffraction tester and a strain micro-tester was used to statistic analyzing variations in microstructure,grain boundary distribution,lattice orientation rotation and grain orientation of Ni-W alloys during in-situ process of uniaxial tensile deformation.A large number of grains in Ni-9%W alloy rotate during deformation process(ε=22%) are divided into sub-grains due to the multiple slip.Because of the strain,the amounts of the high angle boundary increases,the twin boundary remarkable decreases and the lattice orientation increase of 15° in the Ni-9%W alloy.The cubic texture of(001) decreases with the increase in the tensile deformation.

【基金】 国家自然科学基金资助项目(No.69936020);军用模拟集成电路国防科技重点实验室基金资助项目(No.51439040203 QT0101)~~
  • 【文献出处】 电子显微学报 ,Journal of Chinese Electron Microscopy Society , 编辑部邮箱 ,2008年06期
  • 【分类号】TG146.15
  • 【下载频次】270
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