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用热水解法制备不同分子质量丝胶粉的溶解性差异及其成因探讨

Solubility of Sericin Powders With Different Molecular Weight Prepared by Hot Water Degradation Method

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【作者】 张海萍周林巨闵思佳丰强高欣汪琦翀朱良均

【Author】 ZHANG Hai-Ping1 ZHOU Lin-Ju2 MIN Si-Jia1 FENG Qiang1 GAO Xin1 WANG Qi-Chong1 ZHU Liang-Jun1*(1Institute of Applied Bioresources,Zhejiang University,Hangzhou 310029,China;2Station of Economical Special Products,Agriculture Bureau of Zhuji City,Zhuji Zhejiang 311800,China)

【机构】 浙江大学应用生物资源研究所诸暨市农业局经济特产站

【摘要】 用沸水法和高温高压热水法提取丝胶溶液,分别在90℃热水中进行二次降解处理,获得具有不同分子质量分布范围的各种热水解丝胶溶液,经冷冻干燥制成丝胶粉。对各种丝胶粉的热水溶解性差异比较和成因探讨表明,热水二次降解能够提高丝胶的水溶性,降解处理时间越长,其水溶性越大;丝胶的分子质量大小能显著影响其溶解性,而丝胶的结晶结构含量对其溶解性的影响较小。研究结果有助于对不同溶解性丝胶的有效利用。

【Abstract】 Sericin solutions were prepared by boiling water extraction method and high temperature and pressure method,then further degraded in hot water(90 ℃).Several kinds of sericin powders with different molecular weight were obtained by freeze drying method from sericin solutions.The difference of hot water solubility of the prepared sericin powders were investigated and the reason was analyzed.The results showed that the solubility was seriously increased with extension of time of hot water treatment.The difference of hot water solubility mainly resulted from the molecular weight distribution of sericin powders,while scarcely affected by the content of crytal structure.

【基金】 国家自然科学基金项目(编号30771633);浙江省科技厅项目(编号2007C13043);诸暨市科研计划项目(编号2007BB34)
  • 【文献出处】 蚕业科学 ,Science of Sericulture , 编辑部邮箱 ,2008年03期
  • 【分类号】TS149
  • 【被引频次】6
  • 【下载频次】177
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