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用比较进样法的Yatay椰子果实精油的GC-MS分析

GC-MS ANALYSIS OF YATAY PALM FRUITS ESSENTIAL OIL USING COMPARATIVE INJECTION METHOD

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【作者】 陆占国; 刘向阳; 苏荣军;

【Author】 LU Zhan-guo1,LIU Xiang-yang2,SU Rong-jun1(1.School of Food Engineering,Harbin University of Commerce,Harbin 150076,China;2.College of Science,Northeast Forestry University,Harbin 150040,China)

【机构】 哈尔滨商业大学食品工程学院; 东北林业大学理化学院; 哈尔滨商业大学食品工程学院 黑龙江哈尔滨150076; 黑龙江哈尔滨150040; 黑龙江哈尔滨150076;

【摘要】 用水蒸汽蒸馏萃取法获得Yatay椰子果实精油,用两种进样方法进行GC-MS分析.用通常进样法检测出88种成分,解析鉴定了占总精油95.11%的65种成分,主要由酯类化合物56.95%,醇18.10%,羧酸14.15%,醛2.73%构成,主成分为己酸乙酯(33.99%).用热解吸进样法检测出105种成分,解析鉴定了占总精油84.43%的60种成分,主要由酯类化合物53.23%,羧酸22.05%,醇3.65%等构成,主成分为月桂酸乙酯(13.83%)和辛酸(13.62%).

【Abstract】 The essential oil was obtained from Yatay palm fruits by water distillation extraction method and was analyzed by GC-MS using two injection method.When used the general injection method,88 constiuents were detected and 65 chemical compounds which occupied 95.11% of total constituents were identified contained esters(56.95%),alcohols(18.10%),carboxylic acids(14.15%),aldehydes(2.73%), and the major constituent was ethyl hexanoate(33.99%).When used the thermal desorption injection method,105 constiuents were detected,and 60 chemical compounds which occupied 84.43% of total constituents were identified contained esters(53.23%),carboxylic acids(22.05%),alcohols(3.65%),the major constituent were ethyl(E)-cinnamate(13.83%) and Octanoic acid(13.62%).

【关键词】 Yatay椰子; 精油; 气相色谱-质谱;
【Key words】 butia yatay becc; essential oil; GC-MS;
  • 【文献出处】 北京工商大学学报(自然科学版) ,Journal of Beijing Technology and Business University(Natural Science Edition) , 编辑部邮箱 ,2008年03期
  • 【分类号】TS255.7
  • 【下载频次】89
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