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蒙药旋覆花挥发油化学成分分析

Study on chemical constituents of volatile oil from Inula japonica Thunb.from Nei Monggol

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【作者】 李增春杨利青徐宁张力侯冬岩

【Author】 LI Zeng-chun~1 YANG Li-qing~1 XU Ning~1 ZHANG Li~1 HOU Dong-yan~21.College of Chemistry,Inner Mongolia University for the Nationalities,Tongliao 028043,China;2.Anshan Normal University,Anshan 114005,China

【机构】 内蒙古民族大学化学学院鞍山师范学院

【摘要】 目的:利用气相色谱-质谱联用技术对蒙药旋覆花挥发油化学成分进行全面分析。方法:使用乙醚萃取浓缩、水蒸气蒸馏的方法提取旋覆花挥发油,利用气相色谱-质谱联用技术分离鉴定,采用 GC 峰面积归一化法定量。结果:共鉴定出29个成分,占挥发油色谱总峰面积的90.35%,其中邻苯二甲酸二丁基酯16.30%,有6个化合物含量超过7%。结论:本方法快速方便,重现性好,适用于旋覆花挥发油化学成分分析。

【Abstract】 Objective:To analyze the chemical components of volatile oil in Inula japonica Thunb.from Nei Monggol by GC-MS.Methods:The volatile oil from inula flower was extracted by ethyl ether,then isolated by steam distil- lation method.Their chemical constituents and relative contents was analyzed by GC-MS method.Results:Twenty nine volatile components of inula flower were separated and identified,which accounted for over 90.35% of total vola- tile oil fraction.In addition,dibutyl phthalate accounted for over 16.30% of total volatile oil fraction and six compounds’ content overpassed 7%.Conclusion:The method is rapid,convenient and reproducible,therefore this method can be applied to the analysis of the volatile oil components,which was extracted from inula flower compo- nents.

【关键词】 旋覆花挥发油气相色谱-质谱
【Key words】 inula flowervolatile oilGC-MS
【基金】 内蒙古教育厅高校科学基金,批准号 ZD0016
  • 【文献出处】 药物分析杂志 ,Chinese Journal of Pharmaceutical Analysis , 编辑部邮箱 ,2007年01期
  • 【分类号】R29
  • 【被引频次】4
  • 【下载频次】256
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