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水蒸汽蒸馏萃取—气相色谱法测定底泥样品中的硝基苯

Determination of Nitrobenzene in Fish Sediment is by Vapor Distill-extraction Gas Chromatograph

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【作者】 玛依努尔丁蕴铮

【Author】 Maynur1,DING Yun-zheng2 (1.Yili Normal University,Yining 835000,Xinjiang;2.Northeast Normal University,Changchun 130024,Jilin,China)

【机构】 伊犁师范学院化学与生物科学学院东北师范大学城市与环境科学学院 新疆伊宁835000吉林长春130024

【摘要】 应用水蒸汽蒸馏萃取—气相色谱法测定了松花江底泥中的硝基苯含量.该方法的最低检出量为0.0016mg/kg,底泥样品中添加硝基苯标准溶液浓度范围为0.502mg/kg~0.0192 mg/kg,测定底泥样品回收率的范围为80.0%~85.3%.实验证明,水蒸汽蒸馏萃取—气相色谱法作为土壤和生物体内硝基苯含量的测定方法,有较低的检出限和比较稳定的回收率.

【Abstract】 The concentration of nitrobenzene in Songhua River sediment was determined by gas chromatograph using vapor distill-extraction.For the method,the lower detection limit was 0.0016 mg/Kg.The standard NB liquates which is added to the sample sediment is about 0.502 mg/kg~0.0192 mg/kg,and the recovery rate extension is about 80%~85.3%.The experiment proved there was lower detection limit and steadier recovery for gas chromatograph using vapor distill-extraction.as a method for the concentration of nitrobenzene being determined in soil and organism.

  • 【文献出处】 伊犁师范学院学报(自然科学版) ,Journal of Yili Normal University(Natural Science Edition) , 编辑部邮箱 ,2007年04期
  • 【分类号】O657.72
  • 【被引频次】6
  • 【下载频次】127
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