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立方氮化硼粉末的热处理研究
Research on the Heat Treatment of Cubic Boron Nitride Powder
【摘要】 将立方氮化硼在氮气或真空中以不同温度和保温时间进行热处理,用XRD和SEM对相组分和形貌进行了分析。结果表明:立方氮化硼在1 350℃氮气氛中经过10 h处理,可以变为六方氮化硼;在1 550℃真空中(1—5 Pa)经过5 h处理,可以变为六方氮化硼,但其粒径和形貌均不发生变化。
【Abstract】 Cubic Boron Nitride powder was heat treated in N2 or in vacuum at different temperatures and dwell time.Its phase composition and morphology were investigated by means of X-ray diffraction(XRD) and scanning electron microscopy (SEM) analysis.Results showed that the cubic Boron Nitride was transformed into hexagonal phase after heat treatment in N2 at 1 350 ℃ for 10 h,or in vacuum(pressure=1—5 Pa) at 1 550 ℃ for 5 h,while no changes occurred in particle size and morphology.
【基金】 新型超硬材料粉末的制备及其超精细加工应用(企业委托项目)
- 【文献出处】 武汉理工大学学报 ,Journal of Wuhan University of Technology , 编辑部邮箱 ,2007年10期
- 【分类号】O613.81
- 【被引频次】7
- 【下载频次】208