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气相色谱-质谱法对水中亚磷酸三乙酯测定方法研究

GC-MS Analysis of Triethyl Phosphit in Water

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【作者】 吕强许莉陈致肖宏展

【Author】 LV Qiang,XU Li,CHEN Zhi,XIAO Hong-zhan(Beijing Institute of Microchemistry,Beijing 100091,China)

【机构】 北京微量化学研究所北京微量化学研究所 北京100091北京100091

【Abstract】 Triethyl Phosphite is the intermediate of producing nervous toxin of organic phosphate,which is involved in the chemicals of schedule 3. in Convention On The Prohibition Of The Development,Production,Stockpiling And Use Of Chemical Weapons And On Their Destruction.A method for the determination of triethyl phosphate was established by GC-MS/SIM.Average recovery was 96.3%-111.5% with linear range between concentration and peak area varying from 0.546-10.928 mg/L and the detection limits were 0.011 ng.

【关键词】 Triethyl phosphiteAnalysisGC-MS
【Key words】 Triethyl phosphiteAnalysisGC-MS
  • 【文献出处】 分析测试学报 ,Journal of Instrumental Analysis , 编辑部邮箱 ,2007年S1期
  • 【分类号】X832
  • 【下载频次】226
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