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防己渗漉工艺的优选研究
Study on the Optimum Percolation Processes of Radix Stephaniae Tetrandrae
【摘要】 目的研究防己渗漉提取的最佳工艺。方法以防己总碱和粉防己碱为考察指标,采用正交实验法对防己的渗漉工艺进行研究。结果确定了最佳工艺条件为浸渍24 h,60%乙醇6倍量渗漉,渗漉速度为快速。结论工艺合理可行,可应用于生产。
【Abstract】 Objective To study the optimum percolation conditions for Radix Stephaniae Tetrandrae.Methods The percolation process of Radix Stephaniae Tetrandrae was studied by orthogonal design,and the content level of total alkaloids and tetrandrine were used as indexes.Results The optimum percolation conditions for Radix Stephaniae Tetrandrae were as follows: the concentration of ethanol was 60 %,the time of soak was 24h,the rate of percolation was 5ml·min-1·kg-1,and the volume of solvent was 6 times.Conclusion The method is reasonable and feasible,and can be applied to batch production.
【关键词】 防己;
渗漉;
正交实验;
总生物碱;
粉防己碱;
【Key words】 Radix Stephaniae Tetrandrae; Percolation; Orthogonal design; Total alkaloids; Tetrandrine;
【Key words】 Radix Stephaniae Tetrandrae; Percolation; Orthogonal design; Total alkaloids; Tetrandrine;
- 【文献出处】 时珍国医国药 ,Lishizhen Medicine and Materia Medica Research , 编辑部邮箱 ,2007年12期
- 【分类号】R283
- 【被引频次】8
- 【下载频次】236