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横向加热石墨炉原子吸收法测定人发中铜含量

Investigation of Conditions in Determining Copper Content in Human Hair by Transversely Headed GF-AAS

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【作者】 阮尚全刘凯邱艳徐丽

【Author】 RUAN Shang-quan QIU Yan LIU Kai XU Li (Department of Chemistry and Life sciences,Neijiang Teachers College,Neijiang,Sichuan 641112,China)

【机构】 内江师范学院化学与生命科学系内江师范学院化学与生命科学系 四川 内江 641112四川 内江 641112

【摘要】 研究了横向加热石墨炉原子吸收光谱法测定人发中铜含量条件.结果表明:以1%的硝酸介质,干燥温度为110℃,灰化温度为900℃,原子化温度为1900℃,铜浓度在0~0.28μg/ml有良好线性关系,r为0.9992,方法检出限为0.013μg/g,用于实际样品分析效果良好,回收率为94.8%~104.2%.在同一体系中能满足FAAS法对Fe,Zn,Ca,Mg的连续测定.

【Abstract】 the condition of the copper content in men’s hair was determined by GF-AAS.The experimental result showed that the linear relation which r was 0.9992,was better in the concentration of the copper of 0~0.28μg/ml,under the conditions of 1% nitric acid as medium,the drying temperature of 110℃,the ashing temperature of 900℃,and the atomization temperature of 1900 C.The detection,limit of the copper of the method is 0. 013μg/g.when the method was used to the analysis of the real samples,the effect was better,and the reclaim was 94. 8%~104.2%.The Content of Fe,Zn,Ca,Mg can be determined by FAAS in the same preprocessing system.

  • 【文献出处】 内江师范学院学报 ,Journal of Neijiang Teachers College , 编辑部邮箱 ,2007年06期
  • 【分类号】R446.1
  • 【被引频次】4
  • 【下载频次】47
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