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间二氯苯水解产物中间苯二酚、间氯苯酚含量的测定
Determination of Resorcinol Purity in the Hydrolysate of m-Dichlorobenzene by High Performance Liquid Chromatography
【摘要】 采用高效液相色谱法测定间二氯苯水解产物中间苯二酚、间氯苯酚的含量,以C18为固定相,V(异丙醇)∶V(水)=80∶20为流动相,检测波长为273 nm。回收率为95.72%~106.84%,相对标准偏差为2.99~5.38(n=7),测定数据重复性好,灵敏度高,变异系数满足分析要求。
【Abstract】 A reversed-phase high performance liquid chromatographic method was used to detect resorcinol and m-chlorophenol.A C18 column was used and mobile phase was V(isopropanol)∶V(water)=80∶20.The wavelength 273 nm was selected.The recoveries were 95.72%-106.84% and the RSD were 2.99-5.38(n=7).
【关键词】 高效液相色谱法;
外标法;
间苯二酚;
间氯苯酚;
【Key words】 high performance liquid chromatography; external standard method; resorcinol; m-chlorophenol;
【Key words】 high performance liquid chromatography; external standard method; resorcinol; m-chlorophenol;
【基金】 中国石化科技开发项目(J205009)
- 【文献出处】 江苏工业学院学报 ,Journal of Jiangsu Polytechnic University , 编辑部邮箱 ,2007年03期
- 【分类号】O657.72
- 【被引频次】1
- 【下载频次】226