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微波消解—原子荧光法测定海洋沉积物中As的研究

Study on determination of As in marine sediments by microwave digestion-atomic fluorescence spectrometry

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【作者】 马新东马永安贺广凯韩庚辰

【Author】 MA Xin-dong1,2,MA Yong-an1,HE Guang-kai1,HAN Geng-chen1 (1.Nationsl Marine Environment Monitoring Center,Dalian 116023,China;2.College of Environment Science and Engineering,Dalian Marine University,Dalian 116026,China)

【机构】 国家海洋环境监测中心国家海洋环境监测中心 辽宁大连116023大连海事大学环境科学与工程学院辽宁大连116026辽宁大连116023

【摘要】 研究了微波消解海洋沉积物中的As,在比较几种不同的酸消解体系后,得到适合海洋沉积物分析的酸消解体系。与传统的湿法消解比较,测试结果无显著性差异。微波消解具有快速高效、试剂用量少、空白值低、样品不易挥发等优点,已成为海洋沉积物样品前处理的有效手段。

【Abstract】 The method of microwave digestion As in marine sediments was studied.The appropriate acid systems were compared with the traditional wet digestion,and the result is not obvious discrepancy.The microwave digestion has many virtues such as high efficiency,less reagent,low blank,less sample volatilization etc,and it has already become an instrumentality to predisposal the marine sediment samples for analysis.

  • 【文献出处】 海洋环境科学 ,Marine Environmental Science , 编辑部邮箱 ,2007年05期
  • 【分类号】O657.31
  • 【被引频次】6
  • 【下载频次】121
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