【摘要】 以多环硼酸化合物异构体为原料,在催化剂钯碳、相转移催化剂四丁基溴化胺的作用下,于碱性条件下,60～68℃反应6～8h,得到多环化合物,收率45%～60%,并用GC-MS、IR、1HNMR、13CNMR确定了其结构。此项脱硼酸技术起到了回收有用原材料、降低多环硼酸的生产成本、减少硼酸生产中的废物排放量的作用。更多还原

【Abstract】 Polycyclic compounds was synthesized from polycyclic-boronic acid under catalyst palladium and phase transfer catalyst at 60~68℃ for 6 to 8 hour with a 45~60% yield. The structure was confirmed by GC-MS,IR,1H NMR and 13C NMR. The method has advantages such as recovering useful raw materials,reducing production costs of polycyclic-boric acid and decreasing wastes release in the process of producing boric acid.更多还原